简介：RapidsolidificationofCu-Pbmonotecticalloyshasbeenaccomplishedduringfreefallina3mdroptube.BothmacrosegregatedanduniformlydispersedstructuresareobservedinCu-40wtpctPballoydroplets,whereasdropletsofcompositionCu-64wtpctPbexhibitonlymacrosegregationmorphologies.Themicrostructuresarestronglydependentondropletsize.Thehigherundercoolingtendstofacilitateliquidphaseseparationandresultsinmoreextensivemacrosegregationinsmallerdroplets.ThereexistsapronouncedtendencyforthePb-richliquidtooccupythesurfaceofthedropletsofbothcompositions,resultingfromthequitelowersurfacetensionofthePb-richphaseandcausingaPb-richlayeratthesurfaceofthesolidifieddroplet.ThenucleationofmonotecticcellsintheCu-40wtpctPbdropletswithdispersedstructurespreferentiallyoccursatthedropletsurface.Asinglenucleationeventtakesplacemorefrequentlyasdropletsizeisreduced.

简介：ThetreatmentoftheGacuncomplexCu-PbbulkconcentratewithhighZn,Ag,etc.,byoxygenpressureacidleachingwasstudied.Theprimarycopperandleadmineralsintheconcentratearetetrahedriteandgalena.Thetreatmentoftetrahedritewasrarelystudied,andmostofsilveroccurredinthemineraltoo.Theoptimumoperatingparametersofoxygenpressureacidleachingwereestablishedbyconditionaltests.Undertheseparameters,theresultofpilotscaletestshowedthattheleachingpercentagesofcopperandzincwereseparatelyashighas98.9wt.％and94.9wt.％,whileleadandsilverweretransformedintosulfateandsulfideprecipitations,respectively.Thecopperandzincinlixiviumwerereclaimedbyextraction-electrowinningandpurification-electrowinning,respectively,andtheleadandsilverintheresiduewerereclaimedseparatelybycarbonatetransformation-silicofluoricacidleachingandthiourealeaching.

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简介：Al-4。5Cu-5Pb合金被扔的沙和寒冷准备。一样的合金也是在1.6MPa的一个煤气的压力扔的水花。微结构特征展览一对为沙和寒冷铸石金的好树枝状的形态学粗糙。Equiaxed谷物被观察因为水花形成了合金。穿测试采用一根大头针--在圆盘上类型安装，揭示更加更低与寒冷和沙铸石金的相比水花穿扔的合金。词法特征在显示的标本和碎片上穿轨道混合oxidative-cum-adhesive为在现在的调查测试的这些合金穿机制。(编辑作者摘要)36个裁判员。

简介：摘要；本设计采用电感耦合等离子发射光谱法（ICP—OES）对岩石样品中的Cu，Pb，Zn，Mn，Ni进行了测定，样品用四酸（）熔矿，不经分离杂质，即可直接测定。该方法选择Cu，Pb，Zn，Mn，Ni的测定分析波长分别为324.7nm，220.3nm,202.5nm,257.6nm,221.6nm分析了用HCl提取与用王水提取,样品首先经磨样机碎至200目,用去离子水湿润后，用四酸熔矿，再将坩埚放置恒温电热板上加热，最后分别用王水或盐酸提取再定容，对其中的Cu，Pb，Zn，Mn，Ni做探究实验。

简介：目的：探讨料姜石对水中Cu、Pb的吸附效果。方法：研究了不同粒径、温度、时间、用量、金属离子浓度等条件下料姜石对水中Cu、Pb吸附效果的影响。结果：料姜石对水中Cu、Pb的吸附效果与粒径、温度、时间、用量基本正相关,随参数的增加,吸附率提高,达到一定量后变化趋势不明显;与金属离子浓度呈负相关,随金属离子浓度的变大,吸附率逐渐降低。结论：本研究对料姜石的物化性能进行了初步评价,结果表明,料姜石对水中部分重金属确实有良好的吸附效果,为制备天然、低成本的新型净水剂提供了新的参考

简介：建立起HNO3-H2O2-HF体系微波消解前处理样品，利用电感耦合等离子体质谱（ICP—MS）同时测定土壤中的铬（Cr）、镍（Ni）、铜（Cu）、砷（As）、铊（Tl）、铅（Pb）6种重金属元素含量的方法。该方法的相关系数在0．9996～1．000，相对标准偏差在0．669％～3．02％，加标回收率为94．68％～115．5％，检出限为2．004～312．4ng／L，结果表明该方法满足重金属分析的要求。用建立起的方法测定了来自湖南、湖北、云南、贵州、河南、福建、辽宁7个省45个产区烟田土壤中的Cr、Ni、Cu、As、田和Pb6种重金属元素含量；与对应烟叶中的6种重金属含量相比，聚类分析结果表明不同省区间土壤中的重金属含量无明显差异，而烟叶中却差异明显。

简介：TheadsorptionkineticsofPb^2+ondifferentsoilsandmineralswithvariablechargeswasstudiedbythetwoion-selectiveelectrodetechniqueatdifferentpHandconcentrations.Theresultsshowedthatmorethan95%ofadsorptiononallthesamplesoccurredduringthefirst5minutes.Alladsorptiontime-dependentdatacouldfitthesurfacesecond-orderequationverywell.ThevaluesofXmweregoethite>kaolinite,andlatosol>redsoilatthesameinitialreactionconcentration.Thevaluesofkwerekaolinite>>goethite,andlatosol>redsoilatthesamereactionpHandinitialconcentration.ThehigherthesuspensionpH,thefastertheadsorptionoccurred.ThemeaningofXmgotbythetwoion-selectiveelectrodetechnique(onekindofbatchtechnique)wasdifferentfromthatbythemiscibledisplacementtechniqueinthattheformerwasonlytheequilibriumadsorptionamountatadefiniteconcentrationandpH,butthelatterwasalmostequaltotheadsorptioncapacityatadefinitepHwithmuchlessinfluenceofconcentration.OnePb^2+wassupposedtooccupytwoadsorptionsitesastheadsorptionmechanismisconcerned.

简介：UltrasonicvelocitieshavebeenmeasuredinsinglephaseBi1.7Pb0.3Sr2CaCu2O8+xandBi1.7Pb0.3Sr2Ca2O10+xpolycrystallinesamples.Anomalouschangesofbothlongitudinalandtransversevelocitieswereobservednear200K,whichindicatesthatsomestructuralphasetransitiomightoccur.Theelasticconstantsofthesesampleshavebeendeterminedfromthemeasuredultrasonicvelocitydata,whicharemuchsmallerthanthoseofYBa2Cu3O7-yandBaTiO3,manifestingthattheinterlayercoup-lingwilldramaticallydecreasewhenthec-axesoftheunitcellsoftheseperovstite-likemultilayerceramicsincrease.ThevaluesofPoissonratio,however,ofthoseceramicsareveryclose,implyingsimilarinteratomicbondingforces.Correctedtovoid-freestate,theDebyetemperatureofthesematerialsisestirnatedas270±20k.ThetemperaturedependenceofDebyetemperaturesforthesematerialsisalsocalculatedbyusingthesamemethodandreportedforthefirsttime.

简介：本文建立了微波消化-原子吸收光谱法测定中成药中Cu、Pb、Hg、As的方法。四种元素方法的相对标准偏差RSD％为2-4.8％,回收率在90～110％之间,定量检出限分别为6.8μgCu/g(干态)、0.41μgPb/g(干态)、0.13μgAs/g(干态)、0.1μgHg/g(干态)。

简介：TheprocesstoobtainhighT（110K）phasequickly,themicrostructureandpropertiesofAg-sheathedBi（Pb）-Sr-Ca-Cu-Osuperconductortapeshavebeenstudied.ItwasfoundthattheformationtimeofthehighTcphasewasgreatlyshortenedbytheadditionofmoreCaandCutothenominalcompositionofBi（Pb）:Sr:Ca:Cu=2:2:2:3andtheadoptionofappropriatesinteringtemperatureandcoolingrate.SuperconductorpowderwithpredominanthighT,phasewaspreparedaftera840C/50htreatment.TheJoftheAg-sheathedtapesandthemagneticfielddependenceofJwereobviouslyimprovedbyrepeatedlypres-singandsintering.Themaximumtransportcurrentdensityat77Kinazeromagneticfieldwas12,200A/cm2.ThemagneticdependenceofJwassummarizedasfollows:6.450A/cm2（B⊥1.B∥S.0.1T）1,810A/cm2（B⊥1.B∥S,1T）,390A/cm2（B⊥1.B∥S,2T）（B:magneticfield.1:electriccurrent.S:surfaceoftapes）.TheimprovementofJwasattributedtotheformationoftheplate-likestructurewithhomogeneouscompositiondistributionandthestrongc-axistexture.

简介：用同步辐射光电子谱详细研究了Cu(111）面上超薄Pb膜随厚度与退火的反应。发现室温下Cu(111）面上亚单层Pb以二维密积岛的形式生长。退火至200℃形成Pb-Cu表面合金。这种表面合金只发生在Cu(111）面的最外的一个原子层。作为在单晶Cu(111)表面诱使薄膜层状生长的活化剂，Pb的表面合金化可能会对它的活化作用产生不利影响。

简介：1主题内容与适用范围受中国微量元素科学研究会委托研究人发、血清的统一分析方法，经一年多专家教授努力工作现予以公布。血清中钙、镁、锌、铁、铜、锰、镉、铅、钴的测定方法。推荐该法，适用于血清中钙、镁、锌、铁、铜、锰、镉、铅、钴的测定。

简介：摘要在分析原子吸收法原理的基础上，本文对原子吸收法在矿石中Zn、Cu、及Pb元素检测中的实际应用问题展开了分析，发现采用该方法可以实现元素含量准确、高效检测。

简介：1主要内容与适用范围本文受中国微量元素科学研究会委托研究人发、血清的统一分析方法，经一年多专家教授努力工作现予以公布。人发中钙、镁、锌、铁、铜、锰、镉、铅、钴的测定方法。推荐该法，适用于人发中钙、镁、锌、铁、铜、锰、镉、铅、钴的测定。

简介：TheTruongSonFoldBelt,locatedatthenortheasternmarginoftheIndochinaBlock,isconsideredtobetectonicallylinkedtothesubductionofthePaleotethysOceanandsubsequentcollision.SeponisoneofthemostimportantsuperlargedepositsoftheTruongSonFoldBelt.OurLA-ICP-MSzirconU-PbdatingresultsshowthatgranodioriteporphyrysamplesfromtheSepondeposithaveagesof302.1-4-2.9Ma,whichisacrucialphaseformagmatic-tectonicalactivitiesfromtheLateCarboniferoustoEarlyPermianandhasavitalinfluenceonthemineralizationofcopperandgold.ZirconfromgranodioriteporphyryyieldsεHf(t)valuesof4.32to9.64,andTDM2hasanaverageageof914Ma,suggestingthatthesourceofthegranodioriteporphyryintheregionweremainlymantlecomponentsbutunderwentmixingandcontaminationofcrustmaterials.TheCe^4+/Ce^3+valueofzirconinthegranodioriteporphyryvarysgreatlyfrom2.4to1438.29,whichshowsmagmamixingmightoccur.Consideringthecharacteristicsoftraceelementsinthezirconandthewholerockgeochemicalcharacteristicsofintrusionrocksaswellasthecharacteristicsofregionalvolcanic-sedimentaryassociation,itisindicatedthatthetectonicsettingmaybethecontinentalarcenvironment.TheSeponAu-Cudepositisderivedfromemplacementofcalc-alkalineintermediate-acidmagmawithcomingfromdeepsourcesinthesubductionprocessofthePaleotethysOcean,formingporphyryMo-Cu,skamCu-Aumineralizationandahydrothermalsedimentary-hostedAumineralizationinthewallrocks.

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简介：用志不分，乃凝于神。你只须专注．奋斗着，猛勇地奋斗着．持续着，永远的持续着，胜利就是你的了。