Crystal Structure of Bis{1-methylthio-1-[1-phenyl-1-（1-phenyl3-methyl-5-oxo-4,5-dihydropyrazol-4-ylene）-methylamino]iminomethyl} Disulfide with the “U” Conformation-中国期刊网

摘要 Thereactionof1-phenyl-3-methyl-4-benzoyl-2,5-dihydro-1H-pyrazol-5-one(PMBP)andmethyldithiocarbazate(mdtc)inmethanolresultsinformationofayellowcrystallinesolid,adductof1-phenyl-3-methyl-4benzoyl-2,5-dihydro-lH-pyrazol-5-oneandmethyldithiocarbazate.Whentheyellowsolidsweredissolvedinamixtureofmethanolandether(1:4),aredcrystal,whichisanoxidationproductoftheformer,wasobtainedbyallowingsolventtoevaporateforafewdaysatroomtemperature.TheX-rayanalysisoftheredcrystalindicatesthatitisanoveldisulfidewithaspecialstructurelikea“U”conformationinthesolidstate.

1ZHANG，Yan;WANG，Qin;等. Synthesis and Antibacterial Activities of 4—Amino—3—（1—aryl—5—methyl—1,2,3—triazol—4—yl）—5—mercapto—1,2,4—triazoles／2—Amino—5—（1—aryl—5—methyl—1,2,3—triazol—4—yl）—1,3,4—.化学,2002-02.
2ZhaoHuiQU;WeiFengSHI;等. Synthesis of 1—（2′—Phenyl）cycloproply1—2,3—epoxypropan—1—ol as the Radical Precursor for the Kinetic Study of Oxiranylcarbinyl Radical.化学,2002-11.
3Jing-Qian Huo;Liu-Yong Ma;Zhe Zhang;Zhi-Jin Fan;Jin-Lin Zhang;Tetyana V. Beryozkina;Vasiliy A. Bakulev. Synthesis and biological activity of novel N-（3-furan-2-yl-1-phenyl-1H-pyrazol-5-yl） amides derivatives.化学,2016-09.
4DING Liyun;YUAN Fang;HUANG Lanfen;HUANG Jun;LIU Xiaofang;LIANG Bing. A Novel Fluorescence Probe 9-（4-（1,2-diamine）benzeneN 1-phenyl）acridine for Nitric Oxide Determination.材料科学与工程,2014-04.
5刘方明;于建新;鲁文杰;刘罡;刘育亭;陈耀祖. Synthesis of heierocyclic compounds from 2-phenyl-1, 2,3-triazole-4-formylhydrazine.化学,1999-01.
6. DETECTION OF INTERMEDIATES IN REACTION BETWEEN N , N’-DI (P-METHYL) PHENYL MONOTHIOXAMIDES AND 1, 3-DIAMINE TRIMETHYLENE USING RAMAN SPECTROSCOPY.化学,1992-07.
7李昶. 2008年1月1日3U8902.管理学,2008-02.
8admin. 1- methyl-4-phenyl-1，2，3，6-tetrahydropyridine对C57BL小鼠行为学及纹状体多巴.医药卫生,2019-04.
9Hua-Quan Liu;De-Cai Wang;Fei Wu;Wei Tang;Ping-Kai Ouyang. Synthesis and biological evaluation of 5＇-phenyl-3＇H-spiro- [indoline-3,2＇-[ 1,3,4]oxadiazol]-2-one analogs.化学,2013-10.
10周静. 1、2、3、4——.教育学,2010-09.

Crystal Structure of Bis{1-methylthio-1-[1-phenyl-1-（1-phenyl3-methyl-5-oxo-4,5-dihydropyrazol-4-ylene）-methylamino]iminomethyl} Disulfide with the “U” Conformation

来源期刊

相关推荐

同分类资源更多

相关关键词

Crystal Structure of Bis{1-methylthio-1-[1-phenyl-1-（1-phenyl3-methyl-5-oxo-4,5-dihydropyrazol-4-ylene）-methylamino]iminomethyl} Disulfide with the “U” Conformation

来源期刊

相关推荐

同分类资源 更多

相关关键词

同分类资源更多